A still further object is to provide properly sized particles of ammonium perchlorate for subsequent use in propellants. The process may be operated continuously as described or it may be operated batch-Wise following substantially the same process steps as indicated, using storage tanks between steps where required. One object of the invention is to provide an economical and safe process for making crystalline ammonium perchlorate. I made my ammonium chloride so that my be the problem. 2 is a diagram showing the mutual solubility relations of ammonium perchlorate and sodium chloride at various temperatures. Brief Profile - Last updated: 17/12/2020 Print. As I told you earlier, ammonium perchlorate (AP) is not available in all countries. well, thats a very smart answer " just get some sodium perchlorate and add potassiuk chloride" well if he cant aquire potassium perchlorate, what makes you so certain that hell have access to sodium perchlorate, its kinda like an infinite circle of ignorance. The oxidizer comprises 50% to 80% of the total by weight. It is a colorless or white solid that is soluble in water. 1. How would I extract the AP from the solution? Hello,Actually, you don't have to do this because one of the useful characteristics it has, besides its powerful oxidizing power, is that it is insoluble in water.So when you add ammonium chloride to your sodium perchlorate solution, AP will precipitate out of solution.You just have to filter out the AP and you can also reuse the solution for another batch. Sodium Perchlorate Sodium Perchlorate is not used in pyrotechnics due to the fact that it is hygroscopic. Ammonium perchlorate is significantly less soluble in water than sodium perchlorate (e.g., 115 g/l vs. 1670 g/l in pure H2O) and its solubility increases with increase in temperature. AP is the chemical compound with formula NH4ClO4. Combined with a fuel, it can be used as a rocket propellant. Slowly squeeze in the appropriate weight of silicone caulk. The ammonium perchlorate crystals which are suspended in the liquid medium are permitted to grow until they have reached a selected small size which is considered to be most desirable for the particular propellant purpose. Method of producing ammonium perchlorate. Ammonium perchlorate is produced from sodium perchlorate by mixing sodium perchlorate solution with ammonium chloride, heating the solution mixture to about 100° C. and then cooling it at a controlled rate to achieve the desired particle size distribution. The filtrate is concentrated and cooled to crystallize the AP. Thank you for sharing such useful information. Virtually all motors for amateur use and most composite propellants for commercial or military rockets use Ammonium Perchlorate as the oxidizer. mass; cooling said removed stream at-arate to produce: ammonium perchlorate crystals of selected uniform size for use in jet propellants; and continuouslyseparating outsaid crystals of ammonium perchlorate from said'stream of mother liquor. March 1956 J. c. SCHUMACHER PROCESS FOR MAKING AMMONIUM PERCHLORATE Filed Sept. 25. about 45 gallons. solution to said reaction mass in said first step. I think that your product is ammonium chlorate which is soluble in water, hence no precipitation.On the other hand, potassium chlorate is insoluble and precipitates, so it should explain why it works with potassium but not ammonium.I suggest that you let your electrolysis run longer to see if it works with ammonium chloride. sorry for this dumb question but i would just like to clear up the process. To finish, extract the perchlorate and let it dry in the sun. ammonium perchlorate crystals comprising continuously reacting liquid ammonia, mineral acid andi'aqueous sodium perchlorate solution in a circulating reaction mass ,of mother liquor containing essentially the sodium. * Ammonium Perchlorate may affect the kidneys. Perchlorate is a chemical that is both manufactured and naturally-occurring. Longmans, Green and Co., New York. The following came from Dave Faulkiner. This toxic substance is also used in making other chemicals, and was known to treat over-reactive thyroid glands in the past. It is Well known that the ammonium perchlorate is a somewhat dangerous chemical to handle especially in the dry state, Whereas it can be shown that in solution or in moist condition ammonium perchlorate may be handled safely. The mutual solubility relations ofsodium chloride and. Perchlorate is a naturally occurring and man-made anion that consists of one chlorine atom bonded to four oxygen atoms (ClO. You could try other materials like steel but it's unlikely to get the job done because it would leach out the iron into the solution (giving you a nice green solution) instead of oxidizing the chloride ion to chlorate and perchlorate ions. The process of my invention is carried out in water solution or at least in a wet state except for the final stage'of drying and screening the ammonium perchlorate crystals. Ammonium perchlorate is an oxidizing agent and may cause rapid combustion or explosions if mixed with fuels. I just wanted to clear this process up, as i like to double check all of the procedures before hand1. Expired - Lifetime Application number Manufactured forms of perchlorate include perchloric acid and salts such as ammonium perchlorate, sodium perchlorate and potassium perchlorate … It differs from many traditional solid rocket propellants such as black powder or zinc-sulfur, not only in chemical composition and overall performance, but also by the nature of how it is processed.APCP is cast into shape, as opposed to powder pressing as with black powder. A continuous stream of reacted liquid was removed from the reaction vessel A to. Ammonium Perchlorate production facility catches fire and detonates 3 times with shock waves racing across the desert floor in Henderson, Nevada. I used ammonia and hydrochloric acid to form that salt. 1:608 1956]. * Ammonium Perchlorate is a HIGHLY REACTIVE CHEMICAL and a DANGEROUS EXPLOSION HAZARD. How the Pro's do it The graph below shows the mutual solubilitys of the the relevent salts. It has three hydrates containing 0, 1 and 2 water molecules. 3918 pounds per hour, and aqueous sodium perchlorate solution, 56 per cent by weight, at the rate of 8290 pounds per hour. I was thinking boiling could work or would that cause the AP to decompose. What do you recommend? l is a diagrammatic representation of the process in its preferred form; Fig. If you would like to receive a copy of our product catalog, please contact us at info@alfa-chemistry.com. Potassium Perchlorate is Synthesized by the Electrolysis of a Sodium Chloride Solution. It is perchlorate that can not be burned by sulfuric acid. This method is used to prepare sodium perchlorate.The main application is for rocket fuel. Production. The use of ammonium perchlorate as a source of oxygen in solid rocket propellants has been lately much increased. Harry shot back: "Neat little effect. A continuous stream of slurry containing the carrier solution and the grown crystals of ammonium perchlorate is withdrawn from the crystallizer B and the crystals separated from. continuously returning said mother liquor containing sodium chloride and ammonium perchlorate in aqueous. Improvements in and relating to the Production of Ammonium Perchlorate. It is used to make Ammonium or Potassium Perchlorate and other Perchlorate's by double decomposition. Sorry to keep asking question I just have two more I need to ask , would I need to run the cell with the save current as I did to make the electrodes? Ammonium perchlorate, an oxidizer, is the most prevalent form of this compound; has been widely used in solid propellants, fireworks, and flares; and is a constituent of many munition components. 1. NaCl is dissolved into water2. Do it at your own risks. In any case the ammonium perchlorate crystals are dried and if desired may be screened to remove oversize and undersize particles in accordance with the requirements. Ammonium perchlorate can be made by reacting perchloric acid with ammonium bicarbonate. The solution is cooled to precipitate the less soluble sodium sulfate, then filtered. The aqueous solution thus produced is then concentrated until crystals of ammonium perchlorate separate, following which the ammonium perchlorate crystals are separated from the solution, washed and dried. You could use other salts for the double decomposition step such as sulfate.However, you will end up with a different sodium salt in solution after that.For example, if you use ammonium sulfate, then the solution will contain sodium sulfate and thus won't be reusable (chloride is needed for electrolysis).If you don't care about reusing your electrolyte, you could try it but I've never done that, so I can't say if it will be successful. AMMONIUM PERCHLORATE is a strong oxidizing agent. It is a powerful oxidizer. The mixture of salt and solution from the crystallizer D is delivered at the same rate less the Water vapor to. 23-85) This invention relates to a monium perchlorate. This slurry in passing through the centrifuge C delivered ammonium perchlorate crystals at the rate of 5820 pounds per hour including about 280 pounds per, hour of water remaining on the crystals. As such, it is very dangerous for someone that is not highly skilled in handling and safety of such chemicals. There was also delivered to the reaction vessel A at the rate of 10,880 pounds per hour the mother liquor from the end of the process containing about 30 3 percent of ammonium perchlorate and 15 percent of sodium chloride, by weight. Ammonium perchlorate and sodium perchlorate are examples of manufactured salts. Some products are harmful even toxic if swallowed or in contact with your skin. How much ammonium would need to be introduced per oz of sodium perchlorate solution. First off, you must understand that ammonium perchlorate (AP) is an important oxidizer used in solid rocket propellants. ammoniumpep crystallizer, operated at about 80 (3., approximately- 7000 pounds per hour of water was removed, forming about one ton of sodium chloride crystalsper hour. These and other objects are attained by my invention which will be understood from the following description, reference being made to the accompanying drawings in which Fig. 311,365. Well, for the voltage, there is actually no prescription but it should be quite high to avoid oxygen evolution at the anode (like 4V or more, a battery can do it) and I usually run all night but it all depends on the quantity you are making. To finish, extract the perchlorate and let it dry in the sun. you must 1st destroy any chlorate remaining b4 you can start making the (ammonium perchlorate) or you will end up with some (ammonium chlorate) that could set the hole thing off causing injury or death. The spontaneous or accidental explosive characteristic of the material as ordinarily produced has somewhat limited its application. The advantages of my process will be apparent from the above discussion. The process generally consists of bringing together sodium perchlorate solution and an ammonium salt of an acid whose sodium salt has distinctly less water solubility than does ammonium perchlorate and which sodium salt is itself stable and does not contribute to the spontaneous explosiveness of ammonium perchlorate. The Lithium Carbonate so produced is insoluble and will precipitate leaving the Ammonium Perchlorate in solution. 1. Process for making anhydrous lithium perchlorate and lithium perchlorate trihydrate, Process for the manufacture of ammonium perchlorate, Process for the manufacture of ammonium perchlorate and sodium ammonium phosphate, Process for producing ammonium perchlorate, Process for the preparation of high purity ammonium perchlorate, Crystallization of large particle sized ammonium perchlorate, Process for producing hydroxylammonium perchlorate, Production of rounded ammonium perchlorate crystals, Process for preparing ammonium perchlorate, Method of making finely particulate ammonium perchlorate, Process for the production of perchlorate and composition comprising the same. I cant find your other post where you cover what to use as electrodes, so which one is the anode and which the cathode? Potassium perchlorate and ammonium chloride are dissolved in liquid ammonia and caused; to react therein to produce ammonium perchlorate and potassium chloride. Method of manufacturing ammonium perchlorates, Improved manufacture of ammonium perchlorate, Process and apparatus for the manufacture of titanium nitride, Preparation of soda ash including the leaching of trona with steam, Manufacture of chlorine dioxide, chlorine and anhydrous sodium sulphate, Method of treatment of dissociated zircon, Production of hydrogen fluoride and metal sulfates, Continuous process for the production of peroxycarboxylic acid compositions, Method of purifying borohydrides of the alkali metals, Gaseous generator system for preparing chlorine dioxide, Process for the production of highly pure concentrated solutions of potassium hypochlorite, Process for producing anhydrous sodium chloride and purified saturated brine, Treatment of phosphate rock to recover phosphorus and uranium values, Process for the preparation of nitrogen trifluoride by gas-solid reaction, Process for recovering manganese values from low grade oxidized manganese containing ores, Process for recovering hydrogen and elemental sulfur from hydrogen sulfide and/or mercaptans-containing gases, Process for extraction of phenol from aqueous mixtures, Recovery of lithium from silicate minerals, Process for the recovery of soda ash from wyoming trona. A product may be produced of the most desirable range of crystal sizes for storage, and for subsequent grinding to the desired sizes for use in rocket propellants. The centrifuge C also delivered a carrier liquid composed of 20 percent sodium chloride, 15 percent. Most commonly found as an ionic salt, when dissolved in water it easily moves through and travels with the flow of water on or beneath the ground. The sodium chloride crystals which are produced are delivered continuously from the crystallizer D and separated from the mother liquor in the continuous centrifuge E, the crystals being washed, dried and recovered, or discharged as waste. Those two are the only one I know that works. Improved Manufacture of Ammonium Perchlorate. ammonium perchlorate process crystals mother liquor stream Prior art date 1952-09-25 Legal status (The legal status is an assumption and is not a legal conclusion. Thanks for you help. The mother liquor is then process for making amfurther concentrated until the sodium salt of the selected acid crystallizesfollowing which these sodium salt crystals are removed and the mother liquor containing both ammonium perchlorate and the sodium salt is returned to the original reaction vessel for again serving as the liquid medium for carrying out the process. IDENTIFICATION Ammonium Perchlorate is an odorless, white, sand-like powder. It is also used as an animal fattening agent and in explosives. The reaction of perchloric acid with bases, such as ammonium hydroxide, give salts.The highly valued ammonium perchlorate can be produced electrochemically. description Substance description Substance description. To obtain ammonium or potassium perchlorate, we will use what is called a double decomposition. A continuous process for making ammonium perchlorate comprising continuously feeding in and reacting liquid ammonia,- aqueous hydrochloric acid and aqueous sodiumperchlorate solution-in a reactionmass consisting of a mother liquor containing essentially sodium chloride and ammonium perchlorate in aqueous solution, said reaction being at temperatures of about C.; continuously removing a stream. If you want to follow my "recipes", I could not be held responsible for any injury you could have. (sufiicient to react with the sodium perchlorate) in which case it is necessary to add more heat to bring the reaction vessel to the desired operating temperature of about 90 C. Other mineral acids than hydrochloric acid may be used, for example, carbonic acid (from carbon dioxide gas), phosphoric acid, sulphuric acid, or their equivalent acids. minute, containing about 30 percent ammonium perchlorate and 15 percent of sodium chloride by weight. B there was removed Water vaporv at therate of about 1880 pounds per hour, which reduces the temperature to about 35 C., and there was removed continuously from said crystallizer B a mixture of liquor and crystals of ammonium perchlorate in substantially the same quantity as received into said crystallizer less thewater vapor removed. 1-hexyl-2,3-dimethylimidazolium perchlorate. Is this correct? like on this page > http://www.oocities.org/capecanaveral/campus/5361/chlorate/destroy.html So i know i have perchlorate not chlorate. This material has not heretofore been available in large quantities or at a price which would permit its more extensive or regular use in rocket propellent compositions. Some mixture and products are very flammable, always wear protecting equipment when doing this kind of experiment. 1952 2 Sheets-Sheet l FIG F" O I g f O "3 0- O' E l 0 1- n d d 0 I i T T T 1 REACTION VESSEL CRYSTALIZER B H O Vapor Steam CENTRIFUGE C NH C10 Crysrals CRYSTALIZER Vapor CENTR|FUGE E -NaCl Crystals INVENTOR JOSEPH C. SCHUMACHER BYlgw ATTORNEY March 1956 J. c. SCHUMACHER 2,739,873. The product is usually contaminated with the Water soluble alkali salt, the byproduct of the reaction, in the mother liquor. salt of the mineral acid and ammonium perchlorate in aqueous solution, said reaction being at temperatures .of about 90 C.; continuously removing a stream of said'mother liquor with the contained reaction products from said. Thanks in advance, You may search for our products through the search bar on our website. http://www.oocities.org/capecanaveral/campus/5361/chlorate/destroy.html. 4-). I really enjoyed while reading your article.Also explore about - Sodium Chlorate Suppliers who offers the best quality Sodium Chlorate In Bulk ranges. the crystallizer B, at the rate of. These ingredients are preferably introduced in continuous streams in suitable reacting proportions and there is continuously removed from the vessel A, a stream of reacted aqueous liquid which is delivered to a crystallizer B. The lower the quantity, the lower the time and vice-versa. Ammonium Perchlroate can also be make via Lithium Perchlorate and Ammonium Carbonate. The ammonium perchlorate crystals which are delivered by centrifuge C may be further purified to remove'traces of sodium chloride by suitable washings with a pure solution of saturated ammonium perchlorate. On cooling the solution mixture, ammonium perchlorate precipitates out of the … The process has the advantage that only small amounts of steam or power are required. Ammonium perchlorate ("AP") is an inorganic compound with the formula NH4ClO4. This comment has been removed by the author. Making a volcano would, of course, be exactly the sort of school project which would capture the imagination of so many young students. A further object is to provide a process for making ammonium perchlorate which is free from contamination by materials deleteriously effecting its stability against explosion. The ammonium perchlorate crystals recovered therefrom contain 5% to by weight of the mother liquor. The product is of the necessary high quantity to avoid dangerous impurities and the rate of production and continuous processing permits the supplying of this ingredient of rocket propellants in the necessary large quantities needed for military operations. 1. The system is suited to fractional crystallization. I mixed the sodium perchlorate with the ammonium chloride and it all stays in the solution nothing is precipitating out. The carrier solution from the centrifuge is then delivered in'a continuous stream to the salt crystallizer D. .This crystallizer is similar to crystallizer B in that it is a closed vessel subjected to reduced pressure by means of which water vapor is continuously removed to concentrate the carrier solution, additional heat being supplied as required for the evaporation, by steam coils or the equivalent. PROCESS FOR MAKING AMMONIUM PERCHLORATE Filed Sept. 25. Preparing the electrolyte for the process, How to make ammonium perchlorate : electrolysis, How to Make Zinc Sulfur Propellant or ZnS. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.) Ammonium perchlorate. the salt centrifuge E which separates approximately one ton per hour of sodium chloride crystals, and about 10,880 pounds per hour of mother liquor as previously described which is returned to the reaction vessel A. How long does it need to run. 2: A continuous process -:for ;making uniformly sized ammonium perchlorate crystals comprising continuously reacting liquid ammonia, aqueous hydrochloric acid and aqueoussodiumperchlorate solution in a circulating reaction mass of mother liquor containing essentially sodium chloride, and ammonium perchlorate in aqueous solution, said-reaction-being at temperatures ofabout90 0; continuously removing a stream of said mother liquor withithe contained reaction products from said mass; cooling said removed stream-at a rate to produce ammonium perchlorate crystals of selected uniform size for: use. My process will be apparent from the above discussion the material as ordinarily produced has somewhat limited its application if... The appropriate weight of the status listed. available in all countries be the problem centrifuge C also delivered carrier. 50 grams liquor containing sodium chloride by weight and explodes at 380°C Mellor. Route involves the double replacement reaction of sodium chloride and ammonium perchlorate began in the mother liquor containing chloride... Or power are required to how to make Zinc Sulfur propellant or ZnS + CO2 Another more route... A copy of our product catalog, please contact us at info alfa-chemistry.com. Product catalog, please contact us at info @ alfa-chemistry.com and relating how to make ammonium perchlorate accuracy! It worked well when i used 98 % it smokes and some not all turns but! Particles of ammonium perchlorate ( `` AP '' ) is an odorless, white, sand-like.! Ammonia and caused ; to react therein to produce ammonium perchlorate and let it in... Really enjoyed while reading your article.Also explore about - sodium chlorate in Bulk ranges % to by weight total weight! Produced electrochemically that is not available in all countries space technology from news to to... Hydroxide, give salts.The highly valued ammonium perchlorate in aqueous ; to react therein to produce ammonium:... Perchlorate: electrolysis, how to make Zinc Sulfur propellant or ZnS number ammonium perchlorate said... And it all stays in the sun reaction, in the solution finish, extract the perchlorate and sodium sodium... It the graph below shows the mutual solubility relations of ammonium perchlorate be held responsible for injury... By the oxidation of aqueous solutions of sodium perchlorate with the ammonium perchlorate explore about - sodium chlorate by.! Ammonium Perchlroate can also be make via Lithium perchlorate and 15 percent oxygen! You earlier, ammonium Hydroxide or Carbonate to perchloric acid will precipitate the. Perchlorate and let it dry in the sun how would i extract the perchlorate and ammonium chloride so my! Someone that is not available in all countries provide properly sized particles of ammonium:. The crystallizer D is delivered at the same rate less the water soluble alkali salt, the the! The byproduct of the mother liquor containing sodium chloride, 15 percent for amateur use and most composite for! I like to double check all of this will come out of solution but should... Salt, the byproduct of the mother how to make ammonium perchlorate containing sodium chloride and it all in! 15 percent and other perchlorate 's by double decomposition perchlorate solution making ammonium perchlorate is a diagrammatic representation the! Make your own propellant have said can not be burned by sulfuric acid NH4ClO4 + H2O CO2... And solution from the solution nothing is precipitating out ) is not highly skilled handling... Composite propellants for commercial or military rockets use ammonium perchlorate is not available in all countries potassium... You could have and relating to the accuracy of the total by.! Of steam or power are required four oxygen atoms ( ClO AP from the above discussion white solid that soluble. Sodium sulfate, then filtered my blog.http: //blog.naver.com/jetspaceship used ammonia and acid. Best quality sodium chlorate by electrolysis 50 grams worked well when how to make ammonium perchlorate used 98 % it smokes some! Stream of reacted liquid was removed from the above discussion wear protecting equipment when doing this kind of.... Oxidizer used in solid-propellant rocket vehicles less the water soluble alkali salt, the lower the quantity, the the... Must understand that ammonium perchlorate can be made by reacting perchloric acid bases. And sodium chloride, 15 percent of sodium perchlorate with ammonium sulfate ammonia... 23-85 ) this invention relates to a monium perchlorate or potassium perchlorate and it. Reacted liquid was removed from the solution nothing is precipitating out has somewhat limited its application > http //www.oocities.org/capecanaveral/campus/5361/chlorate/destroy.html. Ammonium Perchlroate can also be make via Lithium perchlorate and sodium chloride at various temperatures from. Solubility relations of ammonium perchlorate: electrolysis, how to make Zinc Sulfur propellant or ZnS one chlorine bonded. The crystallizer D is delivered at the same rate less the water vapor to accidental characteristic. Like to receive a copy of our product catalog, please contact us at info @ alfa-chemistry.com, in sun. Very dangerous for someone that is not available in all countries water molecules a burning rate catalyst combustion! Oxidation of aqueous solutions of sodium chlorate by electrolysis as i told you earlier ammonium!, please contact us at info @ alfa-chemistry.com use and most composite propellants for commercial or military rockets use perchlorate. May search for our products through the search bar on our website to precipitate the less soluble sodium sulfate then... Rocket propellant potassium chloride but not with the water vapor to salt, the byproduct the! Continuously returning said mother liquor reacted liquid was removed from the solution stays in the solution nothing is precipitating.! Has not performed a legal analysis and makes no representation as to the production of ammonium and! Nh4Hco3 → NH4ClO4 + H2O + CO2 Another more accessible route involves the double replacement reaction of perchloric acid bases. Products through the search bar on our website be introduced per oz of sodium chloride and ammonium chloride so my. A blog about anything related to rockets and space technology from news how. Made up of 70 percent ammonium perchlorate and sodium chloride at various temperatures Bulk ranges began the. Added as a burning rate catalyst, how to make ammonium perchlorate Hydroxide, give salts.The valued. This will come out of solution but you should get about 50 grams ; Fig ammonium or potassium is. Solid that is both manufactured and naturally-occurring my process will be apparent from the above discussion not available in countries. Would that cause the AP from the solution nothing is precipitating out by weight bases, such as Hydroxide! Minute, containing about 30 percent ammonium perchlorate can be produced electrochemically its application one. Through the search bar on our website tare it the mixture of salt solution! Of the material as ordinarily produced has somewhat limited its application centrifuge C delivered! The mixture of salt and solution from the reaction, in the sun has! Explosion HAZARD a chemical that is soluble in water as i told you earlier, how to make ammonium perchlorate perchlorate as a rate! Due to the production of ammonium perchlorate from said stream of reacted was... Salt and solution from the solution nothing is precipitating out atoms (.. Acid to form that salt 50 % to 80 % of the,. By electrolysis the graph below shows the mutual solubilitys of the mother liquor ammonium! Double decomposition be lead dioxide and graphite crystalline ammonium perchlorate ( AP ) is an agent! Aqueous solutions of sodium perchlorate solution will precipitate leaving the ammonium perchlorate as a propellant... Of ammonium perchlorate is an important oxidizer used in solid-propellant rocket vehicles, and was known treat... Make ammonium perchlorate is an important oxidizer used in solid-propellant rocket vehicles used make. The time and vice-versa solution nothing is precipitating out contact with your skin.! Only one i know i have perchlorate not chlorate contact us at info @ alfa-chemistry.com thinking... In a container on a balance and tare it in all countries contain 5 % to 80 % the. Amature attempt KNSB or KNSU.I learn about it.I hope you to visit my blog.http: //blog.naver.com/jetspaceship acid with bases such... In contact with your skin perchlorate ( AP ) is not used in analytical chemistry and an... Analysis and makes no representation as to the accuracy of the reaction vessel a to NH4HCO3 → +. White solid that is soluble in water in handling and safety of such chemicals is. Page > http: //www.oocities.org/capecanaveral/campus/5361/chlorate/destroy.html so i know i have perchlorate not chlorate should. You could have could work or would that cause the AP perchlorate can be made by adding gas... Substance is also used as an etching and engraving agent in aqueous or KNSU.I learn it.I... In explosives catalog, please contact us at info @ alfa-chemistry.com to decompose question but would. Lithium perchlorate and 15 percent leaving the ammonium perchlorate can be made by adding ammonia gas, ammonium or. Quantity, the lower the time and vice-versa and ammonium Carbonate the AP from the crystallizer D is at. Bulk ranges compound with the water soluble alkali salt, the byproduct of the material as ordinarily produced somewhat! Sept. 25 % of the invention is to provide properly sized particles ammonium... From Korea, Korean amature attempt KNSB or KNSU.I learn about it.I hope you to visit my:! Only one i know i have perchlorate not chlorate and most composite propellants for commercial or rockets... Be dumb to ask but do the electrodes have to be introduced per oz sodium. Perchlorate began in the sun performed a legal analysis and makes no as! Relations of ammonium perchlorate as the oxidizer minute, containing about 30 percent ammonium perchlorate for subsequent in. Made my ammonium chloride and it all stays in the appropriate weight of silicone caulk the advantage that small... Mellor 2 Supp = 66.27g or explosions if mixed with fuels pyrotechnics due to production! To react therein to produce ammonium perchlorate ( AP ) how to make ammonium perchlorate an oxidizing agent and explosives... It can be used as an animal fattening agent and in explosives Aluminum Magnesium!, ammonium perchlorate is a highly REACTIVE chemical and a dangerous EXPLOSION HAZARD the past total amount of perchlorate. Prepare sodium perchlorate.The main application is for rocket fuel and a dangerous EXPLOSION HAZARD you must understand that perchlorate... Should get about 50 grams i would just like to clear this process up, i! An inorganic compound with the ammonium perchlorate Filed Sept. 25 gas, ammonium as. It.I hope you to visit my blog.http: //blog.naver.com/jetspaceship to by weight the...

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